Metallurgical AnalysisMcGraw-Hill Book Company, Incorporated, 1924 - 472 sider |
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Side 7
... strong canvas cloth is placed beneath the area thus marked off , and spread upon the mine floor to receive the sample , which is procured with a pick by cutting the coal , start- ing preferably at the bottom , from between the two ...
... strong canvas cloth is placed beneath the area thus marked off , and spread upon the mine floor to receive the sample , which is procured with a pick by cutting the coal , start- ing preferably at the bottom , from between the two ...
Side 19
... strong a solution of ammonium and sodium salts that the pre- cipitation of the magnesium phosphate will not take place promptly . However , the precipitation will be complete in time . To get rid of the ammonium salts , the filtrate may ...
... strong a solution of ammonium and sodium salts that the pre- cipitation of the magnesium phosphate will not take place promptly . However , the precipitation will be complete in time . To get rid of the ammonium salts , the filtrate may ...
Side 20
... strong HCl , evaporating to dryness to dehydrate any soluble silica and then filtering off , washing and weighing the residue . Iron and alumina , lime and magnesia are then determined in the filtrate as in the filtrate from the silica ...
... strong HCl , evaporating to dryness to dehydrate any soluble silica and then filtering off , washing and weighing the residue . Iron and alumina , lime and magnesia are then determined in the filtrate as in the filtrate from the silica ...
Side 25
... strong solution of MnSO4 are added to the liquid before titration . As the titration proceeds , rapid effervescence of CO2 takes place , resulting in a spraying out of some of the liquid unless the titration is done in a flask ...
... strong solution of MnSO4 are added to the liquid before titration . As the titration proceeds , rapid effervescence of CO2 takes place , resulting in a spraying out of some of the liquid unless the titration is done in a flask ...
Side 29
... strong , as it will likely be , dilute the calculated amount and titrate again . Note . Hydrochloric acid makes the best standard acid for general use because it forms readily soluble salts with all the radicals commonly titrated with ...
... strong , as it will likely be , dilute the calculated amount and titrate again . Note . Hydrochloric acid makes the best standard acid for general use because it forms readily soluble salts with all the radicals commonly titrated with ...
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Metallurgical Analysis Nathaniel Wright Lord,Dana James Demorest Ingen forhåndsvisning tilgjengelig - 2015 |
Vanlige uttrykk og setninger
absorbed acetate acid solution added alkaline aluminium ammonia ammonium analysis antimony apparatus arsenic asbestos assay beaker bismuth bottle bulb burette c.c. of HCl c.c. of HNO3 c.c. of strong c.c. of water calcium calorimeter cent Chem chloride chromium coal coke color combustion containing cool copper crucible cubic centimeters cupel determination dilute dissolved drop end point evaporate to dryness excess ferric ferrous sulfate filter and wash filter paper filtrate flask fumes furnace fusion glass gram heat to boiling hot water hydrochloric acid hydrogen sulfide hydroxide ignite iodine iron lead liquid manganese mercury metal method minutes MnO2 NaOH naphthalene NH4OH nickel nitric acid obtained oxide oxygen permanganate phosphorus pipette platinum potassium present reagent removed residue rubber salts sample silica silver SiO2 slag small amount sodium carbonate soluble standard steel stirring stopper sulfuric acid temperature tion titanium titration tube vanadium volume weigh zinc
Populære avsnitt
Side xii - The total pressure exerted by a mixture of gases is equal to the sum of the partial pressures of the gases in the mixture.
Side 184 - Without interrupting the current, siphon off the acid solution, at the same time filling the beakers with distilled water. Remove the cathodes quickly and rinse them in distilled water and two successive baths of alcohol. An experienced operator can quickly remove a cathode and immerse it in water without loss. Throw off the excess alcohol by a quick motion of the hand and ignite the remainder by bringing the cathode quickly to the flame of an alcohol lamp; then keep the cathode moving continually...
Side 280 - C. require larger proportions of air to gas; however, a strongly reducing atmosphere is not so essential at the higher temperatures, as refractory ashes, owing to their low iron-oxide content, are only slightly affected by oxidizing or reducing atmospheres. After a test has been completed, turn the supply of gas and air off gradually to avoid cracking the muffle crucible. The softening temperature is...
Side 279 - While such a flame is maintained above the furnace, gradually increase the temperature by a suitable adjustment of gas and air to 800° C., then reduce the rate of heat increase to not less than 5° C. and not more than 10° C. per minute. Maintain this rate until the end of the test. It is also important that the 6-in.
Side 279 - Fig. 2, place the loosely fitting cover g on the crucible, and ignite the gas. It is necessary to let the gas burn about 10 minutes to heat the furnace parts before the large cover plate of the furnace is replaced; otherwise the flame is apt to blow out. During this time increase the flow of gas and air sufficiently to cause the combustion to take place just above the tuyeres and yet maintain a yellowish flame at least 6 in.
Side 277 - ... from the top of the cylinder (excluding cover plate), and a 1-in. thermocouple hole 90 deg. to the right of the observation hole; the bottom of these two holes being in the same horizontal plane. The interior of the furnace is cylindrical and approximately 7 in. in diameter and 1 1 in.
Side 278 - ... the bottom of the crucible, and a thermocouple hole 1 in. in diameter, 90 deg. to the right of the observation hole. The bottom of this hole should be in the same horizontal plane as the bottom of the observation hole.
Side 264 - After the more rapid discharge of volatile matter has subsided, as shown by the disappearance of the luminous flame, tap the cover lightly to more perfectly seal the crucible and thus guard against the admission of air.
Side 264 - C. ± 20° C. in the crucible, as shown by a thermocouple kept in the furnace. If the determination of volatile matter is not an essential feature of the specifications under which the coal or coke is bought, a Meker burner may be used. Method For Coal and Coke, Usual Method : Weigh 1 g.
Side 415 - HC1, evaporated nearly to dryness, taken up with cold water, and any residual matter is filtered off. The solution is then boiled with oxalic acid until the gold is all precipitated. It is well to let the solution stand overnight before filtering off the gold. The gold is filtered off and the platinum, recovered by boiling the solution, which has first been neutralized with sodium carbonate, with formic acid, is then filtered off, ignited, and its weight added to that of the platinum already found....