Metallurgical AnalysisMcGraw-Hill Book Company, Incorporated, 1924 - 472 sider |
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Side v
... titration are entirely new . The chapters on water analysis , analysis of alloy steels and gas analysis have been almost entirely rewritten . Nearly all of the methods described in these and other chapters have been used many times in ...
... titration are entirely new . The chapters on water analysis , analysis of alloy steels and gas analysis have been almost entirely rewritten . Nearly all of the methods described in these and other chapters have been used many times in ...
Side xvi
... titration by arsenite or ferrous solutions and the colorimetric process are described . PAGE 72 CHAPTER VII THE DETERMINATION OF SULFUR . The determination of sulfur in iron ores , pyrite ores , etc. and in iron and steel by gravimetric ...
... titration by arsenite or ferrous solutions and the colorimetric process are described . PAGE 72 CHAPTER VII THE DETERMINATION OF SULFUR . The determination of sulfur in iron ores , pyrite ores , etc. and in iron and steel by gravimetric ...
Side xvii
... titration after purification of the WO3 and with or without fusion of the sample . The precipitation of Tungsten by Cinchonine . CHAPTER XIII 138 THE DETERMINATION OF MOLYBDENUM IN STEELS , FERRO ALLOYS AND ORES . . . . . 142 Molybdenum ...
... titration after purification of the WO3 and with or without fusion of the sample . The precipitation of Tungsten by Cinchonine . CHAPTER XIII 138 THE DETERMINATION OF MOLYBDENUM IN STEELS , FERRO ALLOYS AND ORES . . . . . 142 Molybdenum ...
Side xix
... titrated with potassium ferro - cyanide or weighed as zinc pyro - phosphate . CHAPTER XXIX THE DETERMINATION OF LEAD IN ORES The electrolytic determination of lead , the lead sulfate method , the permanganate titration and the ...
... titrated with potassium ferro - cyanide or weighed as zinc pyro - phosphate . CHAPTER XXIX THE DETERMINATION OF LEAD IN ORES The electrolytic determination of lead , the lead sulfate method , the permanganate titration and the ...
Side xx
... titration with iodine after being separ- ated from antimony by distillation as chloride . Antimony is deter- mined by titration of the arsenic free residue by permanganate after reduction with the antimony in hot sulfuric acid . CHAPTER ...
... titration with iodine after being separ- ated from antimony by distillation as chloride . Antimony is deter- mined by titration of the arsenic free residue by permanganate after reduction with the antimony in hot sulfuric acid . CHAPTER ...
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Metallurgical Analysis Nathaniel Wright Lord,Dana James Demorest Ingen forhåndsvisning tilgjengelig - 2015 |
Vanlige uttrykk og setninger
absorbed acetate acid solution added alkaline aluminium ammonia ammonium analysis antimony apparatus arsenic asbestos assay beaker bismuth bottle bulb burette c.c. of HCl c.c. of HNO3 c.c. of water calcium calorimeter cent Chem chloride chromium coal coke color combustion containing cool copper crucible cubic centimeters cupel determination dilute dissolved drop end point evaporate to dryness excess ferric ferrous sulfate filter and wash filter paper filtrate flask fumes furnace fusion glass gram heat to boiling hot water hydrochloric acid hydrogen sulfide hydroxide ignite iodine iron lead liquid liter manganese mercury metal method minutes MnO2 NaOH naphthalene NH4OH nickel nitric acid obtained oxide oxygen permanganate phosphorus pipette platinum potassium present reagent removed residue rubber salts sample silica silver SiO2 slag small amount sodium carbonate soluble standard steel stirring stopper sulfuric acid temperature tion titanium titration tube vanadium volume weigh wire zinc
Populære avsnitt
Side xii - The total pressure exerted by a mixture of gases is equal to the sum of the partial pressures of the gases in the mixture.
Side 184 - Without interrupting the current, siphon off the acid solution, at the same time filling the beakers with distilled water. Remove the cathodes quickly and rinse them in distilled water and two successive baths of alcohol. An experienced operator can quickly remove a cathode and immerse it in water without loss. Throw off the excess alcohol by a quick motion of the hand and ignite the remainder by bringing the cathode quickly to the flame of an alcohol lamp; then keep the cathode moving continually...
Side 280 - C. require larger proportions of air to gas; however, a strongly reducing atmosphere is not so essential at the higher temperatures, as refractory ashes, owing to their low iron-oxide content, are only slightly affected by oxidizing or reducing atmospheres. After a test has been completed, turn the supply of gas and air off gradually to avoid cracking the muffle crucible. The softening temperature is...
Side 279 - While such a flame is maintained above the furnace, gradually increase the temperature by a suitable adjustment of gas and air to 800° C., then reduce the rate of heat increase to not less than 5° C. and not more than 10° C. per minute. Maintain this rate until the end of the test. It is also important that the 6-in.
Side 279 - Fig. 2, place the loosely fitting cover g on the crucible, and ignite the gas. It is necessary to let the gas burn about 10 minutes to heat the furnace parts before the large cover plate of the furnace is replaced; otherwise the flame is apt to blow out. During this time increase the flow of gas and air sufficiently to cause the combustion to take place just above the tuyeres and yet maintain a yellowish flame at least 6 in.
Side 277 - ... from the top of the cylinder (excluding cover plate), and a 1-in. thermocouple hole 90 deg. to the right of the observation hole; the bottom of these two holes being in the same horizontal plane. The interior of the furnace is cylindrical and approximately 7 in. in diameter and 1 1 in.
Side 278 - ... the bottom of the crucible, and a thermocouple hole 1 in. in diameter, 90 deg. to the right of the observation hole. The bottom of this hole should be in the same horizontal plane as the bottom of the observation hole.
Side 264 - After the more rapid discharge of volatile matter has subsided, as shown by the disappearance of the luminous flame, tap the cover lightly to more perfectly seal the crucible and thus guard against the admission of air.
Side 264 - C. ± 20° C. in the crucible, as shown by a thermocouple kept in the furnace. If the determination of volatile matter is not an essential feature of the specifications under which the coal or coke is bought, a Meker burner may be used. Method For Coal and Coke, Usual Method : Weigh 1 g.
Side 415 - HC1, evaporated nearly to dryness, taken up with cold water, and any residual matter is filtered off. The solution is then boiled with oxalic acid until the gold is all precipitated. It is well to let the solution stand overnight before filtering off the gold. The gold is filtered off and the platinum, recovered by boiling the solution, which has first been neutralized with sodium carbonate, with formic acid, is then filtered off, ignited, and its weight added to that of the platinum already found....