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New Books: A Brief Course in Qualitative Analysis; Alkaloidal Estimation; Traité d'Analyse des Substances Minérales; A Textbook of Elementary Analytical Chemistry, Qualitative and Volumetric; Lighting by Acetylene; A Short Course in Inorganic Qualitative Analysis for Engineering Students.. Books Received

889

897

DECEMBER.

A New Gas. By Charles F. Brush..................

On the Facilities for Standardizing Chemical Apparatus Afforded by
Foreign Governments and Our Own. By Louis A. Fischer...
The Cyclical Law of the Elements. By Thomas Bayley....
Atomic Volume as a Periodic Function. By Thomas Bayley.......
The Oil of Corn. By C. G. Hopkins..

899

912

927

935

948

Some Errors in the Determination of Nitrogen.
A Condenser for Extraction Work. By C. G. Hopkins................

By C. G. Hopkins. 961

965

Review: Some Records of the Year's Progress in Applied Chemistry 967

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MA

OF SOLUTIONS.

BY L. M. DENNIS.

Received November 10, 1897.

ANY forms of dischargers for examining the spark spectra of solutions have been described, but all of those with which the writer is acquainted possess disadvantages that seriously impair their value.

To prevent the spattering of the liquid upon the slit of the spectroscope the terminals are, in some cases, surrounded by a glass tube. If a spark of even moderate intensity be used, the liquid which is thrown against the walls of the tube soon cuts off most of the light and obscures the spectrum. It is then necessary to disconnect the discharger and to thoroughly clean the walls of the tube, an operation wasteful both of time and material. Others recommend that the glass tube be abandoned and that free terminals be employed. In this case it becomes necessary to place the spectroscope at some distance from the discharger to avoid the spattering of the liquid against the slit. Again, if the observations are at all prolonged, the liquid in the discharger is soon used up to such an extent that the lower terminal becomes too dry to give a brilliant spectrum. The discharger

must then be refilled.

These difficulties are obviated by the following device which we have been using for the past year. No striking originality

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